Ethyl xanthate → HCID 88781480, compound

HRID 918575Notes

Reaction equation

HRID 918575 reaction equation
Cl[CH2:2][C:3]1[CH:8]=[N:7][C:6]([CH3:9])=[C:5]2[O:10][C:11](=[O:14])[O:12][CH2:13][C:4]=12.CCOC(S)=[S:19]>>[SH:19][CH2:2][C:3]1[CH:8]=[N:7][C:6]([CH3:9])=[C:5]2[O:10][C:11](=[O:14])[O:12][CH2:13][C:4]=12

Participants

3

Reactant 2

HCID 8823Ethyl xanthateHCID 70588340HCID 70588340, compound

Product 1

HCID 88781480HCID 88781480, compound

Procedure

5-Chloromethyl-8-methyl-2-oxo-4H-m-dioxino-[4,5-c]pyridine is converted to the corresponding ethyl xanthogenate and reduced in accordance with the procedure of Example 19, Step B, to give 5-mercaptomethyl-8-methyl-2-oxo-4H-m-dioxino[4,5-c]pyridine.

Sources & evidence

ORD record
ord-1aaa69e7f29e4917b80e514a691fd67a
Source dataset
uspto-grants-1976_07
Patent number
US03971797

Reaction notes

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