HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Bromo-3-phenylpropanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Bromo-3-phenylpropanoic acid | HCID 167544 | — |
| Product | 2-Bromo-3-phenylpropanoyl chloride | HCID 263031 | — |
Reaction Steps
60.5g of 2-bromo-3-phenylpropionic acid was mixed with 100 ml of thionylchloride and the mixture was refluxed for 3 hours and, after the excess thionylchloride had been distilled off, was distilled under reduced pressure to give 46.2g of 2-bromo-3-phenylpropionylchloride. (b.p. 100°- 101°C/4 mmHg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971828 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-143360e4a8474e3e9dbcd89db64d2196 |
| Source note | uspto-grants-1976_07 |