HCID 21506010, compound → HCID 21506155, compound

HRID 918615Notes

Reaction equation

HRID 918615 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[C:11]([S:21](=[O:24])(=[O:23])[NH2:22])[C:12]=1[NH:13][C:14]1[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][CH:15]=1)[C:7]([OH:9])=[O:8])([O-])=O.N(C1C(S(=O)(=O)N)=CC(C(O)=O)=CC=1[N+]([O-])=O)C1C=CC=CC=1>>[NH2:1][C:4]1[CH:5]=[C:6]([CH:10]=[C:11]([S:21](=[O:24])(=[O:23])[NH2:22])[C:12]=1[NH:13][C:14]1[CH:15]=[CH:16][C:17]([CH3:20])=[CH:18][CH:19]=1)[C:7]([OH:9])=[O:8]

Participants

3

Reactant 2

HCID 21506010HCID 21506010, compoundHCID 215060714-Anilino-3-nitro-5-sulphamyl-benzoic acid

Product 1

HCID 21506155HCID 21506155, compound

Procedure

By substituting 3-nitro-5-sulphamyl-4-(p-toluidino)-benzoic acid for the 4-anilino-3-nitro-5-sulphamyl-benzoic acid of Example 9 B, the above compound was obtained with a melting point of 249°-252°C.

Workup

  1. customthe above compound was obtained with a melting point of 249°-252°C.

Sources & evidence

ORD record
ord-2d70c1f6214642959dba50a213fc8c47
Source dataset
uspto-grants-1976_07
Patent number
US03971819

Reaction notes

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