HCID 21506059, compound → HCID 21506000, compound

HRID 918636Notes

Reaction equation

HRID 918636 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[NH:11][C:12]1[C:20]([S:21](=[O:24])(=[O:23])[NH2:22])=[CH:19][C:15]([C:16]([OH:18])=[O:17])=[CH:14][C:13]=1[N+:25]([O-])=O.N(C1C(S(=O)(=O)N)=CC(C(O)=O)=CC=1[N+]([O-])=O)C1C=CC=CC=1>>[NH2:25][C:13]1[CH:14]=[C:15]([CH:19]=[C:20]([S:21](=[O:24])(=[O:23])[NH2:22])[C:12]=1[NH:11][C:2]1[CH:3]=[CH:4][C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[CH:1]=1)[C:16]([OH:18])=[O:17]

Participants

3

Reactant 2

HCID 21506059HCID 21506059, compoundHCID 215060714-Anilino-3-nitro-5-sulphamyl-benzoic acid

Product 1

HCID 21506000HCID 21506000, compound

Procedure

By substituting 4-(β-naphthylamino)-3-nitro-5-sulphamyl-benzoic acid for the 4-anilino-3-nitro-5-sulphamyl-benzoic acid of Example 9 B, the above compound was obtained with a melting point of 245°C.

Workup

  1. customthe above compound was obtained with a melting point of 245°C.

Sources & evidence

ORD record
ord-50ab8052845f43feb8f6cff7154721ec
Source dataset
uspto-grants-1976_07
Patent number
US03971819

Reaction notes

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