HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21506004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 21506055 | HCID 21506055 | — |
| Product | HCID 21506004 | HCID 21506004 | — |
Reaction Steps
A mixture of 3-amino-4-(4-benzyloxyphenoxy)-5-sulphamyl-benzoic acid (4 g), benzyl bromide (4.1 g), and ethanol (60 ml) was refluxed for 4 hours. After cooling, the precipitated ethyl 3-benzylamino-4-(4-benzyloxyphenoxy)-5-sulphamyl-benzoate was isolated by filtration and recrystallized from ethanol. The compound was obtained with a melting point of 166°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971819 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-bc964b3aaff64c41b4e8a83c3a3fb73e |
| Source note | uspto-grants-1976_07 |