HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Ethylthio)aniline → HCID 118204261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Ethylthio)aniline | HCID 10149009 | — |
| Reactant | 2-Nitro-4-(trifluoromethyl)benzaldehyde | HCID 11160305 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 118204261 | HCID 118204261 | 96.3% |
Reaction Steps
A mixture of 500 mg of 2-nitro-4-trifluoromethylbenzaldehyde, 349 mg of 2-(ethylsulfanyl)aniline and 4 ml of toluene was refluxed for 4 hours and then concentrated under reduced pressure. The resulting residue was washed with t-butyl methyl ether to obtain 777 mg of (2-ethylsulfanylphenyl) (2-nitro-4-trifluoromethylbenzylidene)amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09271500B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-d792b151c9554b06a958cb3a92d649c3 |
| Source note | uspto-grants-2016_03 |