4-Methylbenzylamine → HCID 118113878, compound

HRID 918863Notes

Reaction equation

HRID 918863 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][NH2:9])=[CH:6][CH:7]=1.[Br:10][C:11]1[CH:12]=[CH:13][C:14]2[N:15]([N:17]=[C:18]([C:20](OCC)=[O:21])[N:19]=2)[CH:16]=1>>[Br:10][C:11]1[CH:12]=[CH:13][C:14]2[N:15]([N:17]=[C:18]([C:20]([NH:9][CH2:8][C:5]3[CH:6]=[CH:7][C:2]([CH3:1])=[CH:3][CH:4]=3)=[O:21])[N:19]=2)[CH:16]=1

Participants

3

Reactant 2

HCID 660354-MethylbenzylamineHCID 68089394ethyl 6-bromo-[1,2,4]triazolo[1,5-a]pyridine-2-carboxylate

Product 1

HCID 118113878HCID 118113878, compound

Procedure

The title compound was prepared by using procedures analogous to those described for the synthesis of Intermediate I, using p-tolylmethanamine and ethyl 6-bromo-[1,2,4]triazolo[1,5-a]pyridine-2-carboxylate as starting materials.

Sources & evidence

ORD record
ord-0c5d1ba2c9a7498ab3fd160f43ada608
Source dataset
uspto-grants-2016_03
Patent number
US09271969B2

Reaction notes

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