2-Bromothiophene-3-carbaldehyde → HCID 67958509, compound

HRID 919080Notes

Reaction equation

HRID 919080 reaction equation
[Br:1][C:2]1[S:3][CH:4]=[CH:5][C:6]=1[CH:7]=[O:8].[C:9]1([CH2:15][CH2:16][CH2:17][Mg]Br)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[Br:1][C:2]1[S:3][CH:4]=[CH:5][C:6]=1[CH:7]([OH:8])[CH2:17][CH2:16][CH2:15][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 122459212-Bromothiophene-3-carbaldehydeHCID 178418471HCID 178418471, compound

Product 1

HCID 67958509HCID 67958509, compound

Procedure

Prepared according to the procedure described in Example 5, Step 1, using the following starting materials: 2-bromo-thiophene-3-carbaldehyde and 3-phenyl-propyl magnesium bromide.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-b4a2be9f2c3f4f748e1f97fcf34af07a
Source dataset
uspto-grants-2016_03
Patent number
US09272990B2

Reaction notes

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