HCID 7019417, compound → HCID 67963767, compound

HRID 919093Notes

Reaction equation

HRID 919093 reaction equation
[Br:1][C:2]1[CH:6]=[N:5][N:4]([CH2:7][CH3:8])[C:3]=1[CH:9]=[O:10].[C:11]1([CH2:17][CH2:18][CH2:19][Mg]Br)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[Br:1][C:2]1[CH:6]=[N:5][N:4]([CH2:7][CH3:8])[C:3]=1[CH:9]([OH:10])[CH2:19][CH2:18][CH2:17][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 7019417HCID 7019417, compoundHCID 178418471HCID 178418471, compound

Product 1

HCID 67963767HCID 67963767, compound

Procedure

Prepared according to the procedure described in Example 5, Step 1, using the following starting materials: 4-bromo-2-ethyl-2H-pyrazole-3-carbaldehyde and 3-phenyl-propyl magnesium bromide.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-ea728a60a5c14cbab94dfd5bc3d1ceb4
Source dataset
uspto-grants-2016_03
Patent number
US09272990B2

Reaction notes

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