Dimethyl Sulfoxide → HCID 86673475, compound

Participants

Reaction Conditions

Reaction Steps

To a 20 mL microwave reaction vial with a micro magnetic stir bar, were added 0.300 g of 1-aminoanthraquinone, 0.207 g of thiourea and 3 mL of DMSO. Then the vial was sealed and heated with microwave at 140° C. for 20 hours. A dark brown gel like mixture was obtained which was purified in a similar fashion with hexane/EtOAc (5:1 to 1:1) as the eluent, and 0.103 g of anthrapyrimidine was obtained, in a yield of 33.0%.

Provenance & Evidence