3-Methoxypropylamine → HCID 71061167, compound

HRID 919271Notes

Reaction equation

HRID 919271 reaction equation
[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12]([OH:14])=O)=[CH:10][CH:9]=2)=[CH:4][C:3]=1[C:17](=[O:25])[NH:18][C:19]1[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=1.[CH3:26][O:27][CH2:28][CH2:29][CH2:30][NH2:31]>>[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12](=[O:14])[NH:31][CH2:30][CH2:29][CH2:28][O:27][CH3:26])=[CH:10][CH:9]=2)=[CH:4][C:3]=1[C:17]([NH:18][C:19]1[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=1)=[O:25]

Participants

3

Reactant 2

HCID 16723-MethoxypropylamineHCID 71061416HCID 71061416, compound

Product 1

HCID 71061167HCID 71061167, compound

Procedure

Reaction of 4-[6-amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid with 3-methoxy-propylamine gives “A94”; method 1: HPLC/MS: 1.30 min, [M+H]=406;

Workup

  1. customgives “A94”
  2. custom1.30 min, [M+H]=406

Sources & evidence

ORD record
ord-bb92cf6ba0414ebebee58f7ee134955b
Source dataset
uspto-grants-2016_03
Patent number
US09273029B2

Reaction notes

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