(2-Methoxyethyl)(methyl)amine → HCID 71060961, compound

HRID 919274Notes

Reaction equation

HRID 919274 reaction equation
[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[C:10]([CH:14]=[CH:15][CH:16]=2)[C:11]([OH:13])=O)=[CH:4][C:3]=1[C:17](=[O:25])[NH:18][C:19]1[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=1.[CH3:26][O:27][CH2:28][CH2:29][NH:30][CH3:31]>>[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][CH:14]=[C:10]([C:11](=[O:13])[N:30]([CH2:29][CH2:28][O:27][CH3:26])[CH3:31])[CH:9]=2)=[CH:4][C:3]=1[C:17]([NH:18][C:19]1[CH:20]=[CH:21][N:22]=[CH:23][CH:24]=1)=[O:25]

Participants

3

Reactant 2

HCID 300977(2-Methoxyethyl)(methyl)amineHCID 710607733-[6-Amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid

Product 1

HCID 71060961HCID 71060961, compound

Procedure

Reaction of 3-[6-amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid with N-(methoxy-ethyl)-methyl-amine gives “A97”; method 1: HPLC/MS: 1.23 min, [M+H]=406;

Workup

  1. customgives “A97”
  2. custom1.23 min, [M+H]=406

Sources & evidence

ORD record
ord-22afe5a412644e5bbe48d759c6895075
Source dataset
uspto-grants-2016_03
Patent number
US09273029B2

Reaction notes

Loading…