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HRID919377

反应详情

EQUATION

反应方程式

HRID 919377 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc([N+](=O)[O-])s1
HCID78281

5-Nitrothiophene-2-carbaldehyde

C5H3NO3S

结构：O=[N+]([O-])c1ccc(C=NNc2nc3ccccc3s2)o1
HCID2856671

未命名化合物

结构：NNc1nc2ccc(OC(F)(F)F)cc2s1
HCID10422158

2-Hydrazinyl-6-(trifluoromethoxy)-1,3-benzothiazole

C8H6F3N3OS

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(C=NNc2nc3ccc(OC(F)(F)F)cc3s2)s1
HCID86664233

未命名化合物

PROCEDURE

实验过程

The compound 3j was prepared according procedure described for 3a by employing 5-nitrothiophen aldehyde (157 mg, 1 mmol) and 2-hydrazino-6-trifluoromethoxy-benzothiazole (249 mg, 1 mmol) at 70° C. for 2 h (yield 219 mg, 75%).

WORKUP

后处理

  1. customat 70° C.
  2. customfor 2 h