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HRID919379

反应详情

EQUATION

反应方程式

HRID 919379 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc([N+](=O)[O-])s1
HCID78281

5-Nitrothiophene-2-carbaldehyde

C5H3NO3S

结构：NNc1nc2ccc(Cl)cc2s1
HCID737197

6-Chloro-2-hydrazinyl-1,3-benzothiazole

C7H6ClN3S

结构：O=[N+]([O-])c1ccc(C=NNc2nc3ccccc3s2)o1
HCID2856671

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(C=NNc2nc3ccc(Cl)cc3s2)s1
HCID86664235

未命名化合物

PROCEDURE

实验过程

The compound 3n was prepared according procedure described for 3a by employing 5-nitrothiophen aldehyde (157 mg, 1 mmol) and 2-hydrazino-6-chloro-benzothiazole (199 mg, 1 mmol) at 70° C. for 2 h (yield 287 mg, 85%).

WORKUP

后处理

  1. customat 70° C.
  2. customfor 2 h