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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 919382Generated: October 26, 2026

2-Benzothiazolinone, hydrazone → N'2-(1,3-benzothiazol-2yl)-5-nitro-2-furanecarbohydrazide

https://huagongshe.com/reaction/919382

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Benzothiazolinone, hydrazoneHCID 11988—
Reactant5-Nitrofuroyl chlorideHCID 90711—
ProductN'2-(1,3-benzothiazol-2yl)-5-nitro-2-furanecarbohydrazideHCID 86664238—

Reaction Conditions

Temperature0 °C

Reaction Steps

The compound 4a was prepared according to above described method by using 5-nitro-2-furancarboxylic acid chloride (300 mg, 1 mmol) and 2-hydrazino-benzothiazole (300 mg, 1.5 mmol) which stirred for 1 h at 0° C. and stirring continued at 25° C. for 11 h (yield 245 mg, 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09273039B2
Source datasetuspto-grants-2016_03
ORD IDord-18a36b4eaac74c44ab0531cb84dbbacf
Source noteuspto-grants-2016_03