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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 919383Generated: November 3, 2026

5-Nitrofuroyl chloride → HCID 86664239, compound

https://huagongshe.com/reaction/919383

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Nitrofuroyl chlorideHCID 90711—
Reactant2-Hydrazinyl-6-methyl-1,3-benzothiazoleHCID 2049839—
ProductHCID 86664239HCID 86664239—

Reaction Conditions

Temperature0 °C

Reaction Steps

The compound 4b was prepared according to above described method by using 5-nitro-2-furancarboxylic acid chloride (300 mg, 1 mmol) and 2-hydrazino-6-methylbenzothiazole (179 mg, 1 mmol) which stirred for 1 h at 0° C. and stirring continued at 25° C. for 11 h (yield 216 mg, 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09273039B2
Source datasetuspto-grants-2016_03
ORD IDord-3bfd09b4841a4114b0b0a92b29d6b188
Source noteuspto-grants-2016_03