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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 919384Generated: October 30, 2026

5-Nitrofuroyl chloride → HCID 86664240, compound

https://huagongshe.com/reaction/919384

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Nitrofuroyl chlorideHCID 90711—
Reactant2-Hydrazinyl-6-methoxy-1,3-benzothiazoleHCID 1987846—
ProductHCID 86664240HCID 86664240—

Reaction Conditions

Temperature0 °C

Reaction Steps

The compound 4c was prepared according to above described method by using 5-nitro-2-furancarboxylic acid chloride (300 mg, 1 mmol) and 2-hydrazino-6-methoxybenzothiazole (260 mg, 1 mmol) which stirred for 1 h at 0° C. and stirring continued at 25° C. for 11 h (yield 283 mg, 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09273039B2
Source datasetuspto-grants-2016_03
ORD IDord-d06a29800b04425181633c9835d97828
Source noteuspto-grants-2016_03