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HRID919389

反应详情

EQUATION

反应方程式

HRID 919389 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc2nc(N)sc2c1
HCID21504

2,6-Benzothiazolediamine

C7H7N3S

结构：Cn1cc([N+](=O)[O-])cc1C(=O)O
HCID2736915

1-Methyl-4-nitro-1H-pyrrole-2-carboxylic acid

C6H6N2O4

PRODUCTS

生成物

1
结构：Cn1cc([N+](=O)[O-])cc1C(=O)Nc1ccc2nc(NC(=O)c3cc([N+](=O)[O-])cn3C)sc2c1
HCID86664245

未命名化合物

PROCEDURE

实验过程

The compound 8b was prepared according to the above described method using compound 7 (165 mg, 1 mmol) and 1-methyl-4-nitro-1H-pyrrole-2-carboxylic acid (340 mg, 2 mmol). Yield 290 mg, 60%; 1H NMR (DMSO-d6) δ 10.9 (bs, 1H, —NH), 8.54 (s, 1H), 7.95 (s, 2H), 7.74-7.71 (m, 2H), 7.50 (s, 2H), 3.96 (s, 6H); ESIMS: m/z 470 (M+H)+.