4-Chlorobenzyl mercaptan → HCID 71236671, compound

HRID 920417Notes

Reaction equation

HRID 920417 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][SH:9])=[CH:4][CH:3]=1.Cl[C:11]1[CH:21]=[C:15]2[N:16]([CH3:20])[CH2:17][CH2:18][CH2:19][N:14]2[C:13](=[O:22])[N:12]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][S:9][C:11]2[CH:21]=[C:15]3[N:16]([CH3:20])[CH2:17][CH2:18][CH2:19][N:14]3[C:13](=[O:22])[N:12]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 804094-Chlorobenzyl mercaptanHCID 717434718-Chloro-1-methyl-3,4-dihydro-1H-pyrimido[1,6-A]pyrimidin-6(2H)-one

Product 1

HCID 71236671HCID 71236671, compound

Procedure

The title compound or its salt was prepared by a procedure similar to that described for E62 starting from (4-chlorophenyl)methanethiol and 8-chloro-1-methyl-3,4-dihydro-1H-pyrimido[1,6-a]pyrimidin-6(2H)-one.

Sources & evidence

ORD record
ord-2a1b433a8d8048279f576a2e624fd70f
Source dataset
uspto-grants-2016_03
Patent number
US09273054B2

Reaction notes

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