Styrene → Decalin
Reaction equation
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]1(S(OCCCCCCCCCCCC)(=O)=O)C=CC=C[CH:10]=1.[Na]>>[CH2:7]1[CH:8]2[CH:3]([CH2:2][CH2:1][CH2:9][CH2:10]2)[CH2:4][CH2:5][CH2:6]1Participants
3
Procedure
Except for changing the amount of the styrene from 150 parts to 100 parts and not using sodium dodecyl benzenesulfonate when performing the polymerization, the same procedure was followed as in Example 6 to obtain a decalin dispersion of the polymer particles J which do not have a core-shell structure. The obtained polymer particles J had an average particle size of 500 nm. Further, except for using the obtained decalin dispersion of polymer particles J not having a core-shell structure, the same procedure was followed as in Example 1 to prepare the slurries and produce the all-solid state secondary cell and the same procedure was followed as in Example 1 to evaluate it. The results are shown in Table 1.
Workup
- customthe polymerization
Sources & evidence
- ORD record
- ord-cd4da5e3e6c1433fb60d81db74b6f339
- Source dataset
- uspto-grants-2016_03
- Patent number
- US09276263B2
Reaction notes
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