HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → sodium 2-[4-[[4-[(2Z)-2-(4-cyanophenyl)-2-methoxyiminoethoxy]phenyl]methoxy]phenyl]cyclopropane-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-[4-[[4-[(2Z)-2-(4-cyanophenyl)-2-methoxyiminoethoxy]phenyl]methoxy]phenyl]cyclopropane-1-carboxylic acid | HCID 56640277 | — |
| Product | sodium 2-[4-[[4-[(2Z)-2-(4-cyanophenyl)-2-methoxyiminoethoxy]phenyl]methoxy]phenyl]cyclopropane-1-carboxylate | HCID 56640581 | 72.4% |
Reaction Steps
Compound 51 was synthesized from sodium hydroxide (0.04 g, 0.96 mmol) and 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylic acid (0.22 g, 0.48 mmol) by following the procedure described in scheme 12 (0.15 g, yield: 72.40%); Purity: 90.60%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-d4ae7da779cf40c885985c6d22d3f629 |
| Source note | uspto-grants-2016_03 |