Ethanol → HCID 87106532, compound

Participants

Reaction Steps

To a solution of ethyl 3-(4′-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}biphenyl-4-yl)propanoate (0.25 g, 0.6 mmol) in THF was added ethanol and aqueous solution of NaOH and stirred at RT for 2 h, reaction mass was concentrated to remove solvents and diluted with water and neutralized with 1 N HCl and extracted with ethyl acetate, organic layer was washed with water and brine solutions dried over anhydrous Na2SO4 and concentrated to white solid (0.2 g, 83.3%); purity: 99.5%

Provenance & Evidence