Triethylamine → HCID 66685338, compound

Participants

Reaction Steps

To a 100 mL RB flask fitted with magnetic stirrer was charged 12 mL THF to the stirred solvent was added 3-(4-{[4-(benzoyloxy)benzyl]oxy}phenyl)propanoic acid (1 g, 2.4 mmol), Ethyl chloroformate (0.36 mL, 38 mmol) and Tri ethyl amine (1.4 mL, 10 mmol) was added −10° C. Then it was stirred at same temp. 45 min then added NH4OH, continued the stirring at same temperature for 1 h. After completion of the reaction (reaction monitored by TLC), reaction mass was extracted with ethyl acetate and water. The organic layer washed with brine and dried by Na2SO4 and evaporated to dryness to get the compound (1 g, Yield: 99%). MS (ESI, 120 eV): m/z=390.2 (M−H)+.

Provenance & Evidence