HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → Methyl (3-(5-(1-(cyclopropylamino)ethyl)-2-methoxypyridin-3-yl)prop-2-yn-1-yl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | Methyl (3-(5-acetyl-2-methoxypyridin-3-yl)prop-2-yn-1-yl)carbamate | HCID 89939692 | — |
| Product | Methyl (3-(5-(1-(cyclopropylamino)ethyl)-2-methoxypyridin-3-yl)prop-2-yn-1-yl)carbamate | HCID 89939691 | — |
Reaction Steps
Methyl [3-(5-acetyl-2-methoxypyridin-3-yl)prop-2-yn-1-yl]carbamate and cyclopropylamine were treated in the similar manner to Reference Example 6(6) to give methyl (3-{5-[1-(cyclopropylamino)ethyl]-2-methoxypyridin-3-yl}prop-2-yn-1-yl)carbamate [Ex(296-3)] as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278944B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-0e95973a2f3f4bfab74fa8ad51847864 |
| Source note | uspto-grants-2016_03 |