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HRID922495

反应详情

EQUATION

反应方程式

HRID 922495 的结构方程式

REACTANTS

反应物

2
结构：CCOC(C)=O.Cl
HCID21866389

未命名化合物

结构：CC(C)(C)OC(=O)N[C@@H]1C[C@H]1c1ccc(NC(=O)c2cccc(Br)c2)cc1
HCID86729828

Carbamic acid, N-[(1R,2S)-2-[4-[(3-bromobenzoyl)amino]phenyl]cyclopropyl]-, 1,1-dimethylethyl ester, rel-

C21H23BrN2O3

PRODUCTS

生成物

1
结构：Cl.N[C@@H]1C[C@H]1c1ccc(NC(=O)c2cccc(Br)c2)cc1
HCID86729829

未命名化合物

PROCEDURE

实验过程

tert-Butyl [trans-2-(4-{[(3-bromophenyl)carbonyl]amino}phenyl)cyclopropyl]carbamate (407 mg) was dissolved in 4N hydrochloric acid/ethyl acetate solution (2 mL), and the mixture was stirred at room temperature for 2 hr. The solvent was evaporated under reduced pressure to give the title compound (320 mg).

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure