HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-(chloromethyl) Dibenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Dibenzofuran-4-ylmethanol | HCID 12373571 | — |
| Product | 4-(chloromethyl) Dibenzofuran | HCID 12373572 | — |
Reaction Steps
Thionyl chloride (6 ml) is added to a solution of Dibenzofuran-4-ylmethanol (0.9 g). The solution is refluxed for 1 hour. Excess of reagent is evaporated to yield 4-(chloromethyl) Dibenzofuran (0.97 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278957B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-3f78c270424e4d93b8c48d249c559dcd |
| Source note | uspto-grants-2016_03 |