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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 922977Generated: October 30, 2026

2-(Methylsulfonyl)ethanamine → HCID 58614737, compound

https://huagongshe.com/reaction/922977

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(Methylsulfonyl)ethanamineHCID 4340561—
Reactant3-Chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acidHCID 66878605—
ProductHCID 58614737HCID 58614737—

Reaction Steps

50 mg of 3-chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid was coupled to 2-(methylsulfonyl)ethanamine via Procedure G. The crude product was purified on reverse phase HPLC to yield 2-chloro-N1-(4-chloro-3-(pyridin-2-yl)phenyl)-N4-(2-(methylsulfonyl)ethyl)terephthalamide. MS (Q1) 492 (M)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09278961B2
Source datasetuspto-grants-2016_03
ORD IDord-9fc323e7595c46f788127de6bf6445a0
Source noteuspto-grants-2016_03