HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-(pyridin-2-yl)aniline → HCID 178522073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-(pyridin-2-yl)aniline | HCID 40151925 | — |
| Reactant | HCID 178524403 | HCID 178524403 | — |
| Reactant | HCID 178524404 | HCID 178524404 | — |
| Product | HCID 178522073 | HCID 178522073 | — |
Reaction Steps
107 mg of a mixture of 4-((4H-1,2,4-triazol-3-ylsulfinyl)methyl)benzoic acid and 4-((4H-1,2,4-triazol-3-ylsulfonyl)methyl)benzoic acid was coupled to 75 mg of 4-chloro-3-(pyridin-2-yl)aniline via Procedure G. The mixture was separated on reverse phase HPLC to give 4-((4H-1,2,4-triazol-3-ylsulfonyl)methyl)-N-(4-chloro-3-(pyridin-2-yl)phenyl)benzamide. MS (Q1) 454.3 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278961B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-7a6ab9081c294c8ea0c6f6566c20a22b |
| Source note | uspto-grants-2016_03 |