HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylpyrazole → HCID 58614888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylpyrazole | HCID 6210 | — |
| Reactant | 4-(Bromomethyl)-N-[4-chloro-3-(2-pyridinyl)phenyl]benzamide | HCID 66878170 | — |
| Product | HCID 58614888 | HCID 58614888 | — |
Reaction Steps
70 mg of 4-(bromomethyl)-N-(4-chloro-3-(pyridin-2-yl)phenyl)benzamide was coupled to 50 mg of 3,5-dimethyl-1H-pyrazole via Procedure P. The reaction was evaporated to dryness and purified by reverse phase HPLC to yield N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-((3,5-dimethyl-1H-pyrazol-1-yl)methyl)benzamide. MS (Q1) 417.3 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278961B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-eda4c226ae40462a84e4ce768940bfcf |
| Source note | uspto-grants-2016_03 |