HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 4-(bromomethyl)-3-(trifluoromethyl)benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 4-Methyl-3-(trifluoromethyl)benzonitrile | HCID 2775598 | — |
| Product | 4-(bromomethyl)-3-(trifluoromethyl)benzonitrile | HCID 58827160 | — |
Reaction Steps
4-Methyl-3-trifluoromethylbenzonitrile is brominated with NBS according to Example 1A to give 4-bromomethyl-3-trifluoromethylbenzonitrile. 1H NMR (400 MHz, CDCl3) δ (ppm) 7.94 (s, 1H), 7.85 (d, J=8.1 Hz, 1H), 7.76 (d, J=8.1 Hz, 1H), 4.63 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278969B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-44bb21c09adb48798f59f1f911a7aaa9 |
| Source note | uspto-grants-2016_03 |