HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-bromobutanimide → 4-Bromomethyl-2,5-dimethoxybenzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | 2,5-Dimethoxy-4-methylbenzonitrile | HCID 595738 | — |
| Produkt | 4-Bromomethyl-2,5-dimethoxybenzonitrile | HCID 58827058 | — |
Reaktionsschritte
2,5-Dimethoxy-4-methylbenzonitrile (4.06 g, 21.5 mmol) is brominates with NBS according to Example 1A to give 4-bromomethyl-2,5-dimethoxybenzonitrile. 1H NMR (400 MHz, CDCl3) δ (ppm) 6.95 (s, 1H), 6.91 (s, 1H), 4.43 (s, 2H), 3.84 (s, 3H), 3.80 (s, 3H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09278969B2 |
| Quelldatensatz | uspto-grants-2016_03 |
| ORD ID | ord-9eb2581263d34e028f14029b877f0e93 |
| Quellennotiz | uspto-grants-2016_03 |