HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorobenzoic Acid → Benzoyl chloride, 3-chloro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorobenzoic Acid | HCID 447 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Benzoyl chloride, 3-chloro- | HCID 69252 | 90% |
Reaction Steps
A solution of 3-chlorobenzoic acid (30 g, 191.61 mmol) in thionyl chloride (200 ml) was stirred overnight at 90° C. The resulting mixture was concentrated under vacuum to afford 3-chlorobenzoyl chloride as light yellow oil (30 g, 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278973B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-e791f0ecd34e44228634a4eef02d6307 |
| Source note | uspto-grants-2016_03 |