HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178513169, compound → 5-(3-chlorophenyl)-4H-1,2,4-triazol-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178513169 | HCID 178513169 | — |
| Solvent | Water | HCID 962 | — |
| Product | 5-(3-chlorophenyl)-4H-1,2,4-triazol-3-amine | HCID 178508290 | 63% |
Reaction Steps
A solution of 2-(3-chlorobenzoyl)hydrazinecarboximidamide (7.8 g, 36.68 mmol) in water (150 ml) was stirred overnight at 90° C. The solids were collected by filtration to afford 3-(3-chlorophenyl)-1H-1,2,4-triazol-5-amine as a off-white solid (4.5 g, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278973B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-a95e77f7619c45a98887aa4b71e0538e |
| Source note | uspto-grants-2016_03 |