HCID 16114856, compound → HCID 59540449, compound

HRID 923391Notes

Reaction equation

HRID 923391 reaction equation
[N+:1]([C:4]1[CH:26]=[CH:25][C:7]([CH2:8][N:9]([CH2:15][C:16]2[CH:21]=[CH:20][C:19]([N+:22]([O-])=O)=[CH:18][CH:17]=2)[C:10]2[CH:14]=[CH:13][O:12][N:11]=2)=[CH:6][CH:5]=1)([O-])=O.[N+](C1C=CC(CN(CC2C=CC([N+]([O-])=O)=CC=2)C2C=CC=CC=2)=CC=1)([O-])=O>>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([CH2:8][N:9]([CH2:15][C:16]2[CH:21]=[CH:20][C:19]([NH2:22])=[CH:18][CH:17]=2)[C:10]2[CH:14]=[CH:13][O:12][N:11]=2)=[CH:25][CH:26]=1

Participants

3

Reactant 2

HCID 16114856HCID 16114856, compoundHCID 59540137HCID 59540137, compound

Product 1

HCID 59540449HCID 59540449, compoundYield 79%

Procedure

The title compound was prepared using the methods from Example 1B substituting the product from Example 33A for the product from Example 1A to provide the title compound (0.32 g, 79% yield).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-513d3ab6bd03461e9e393f57468f3d6e
Source dataset
uspto-grants-2016_03
Patent number
US09278922B2

Reaction notes

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