HCID 16114856, compound → HCID 59540448, compound

HRID 923394Notes

Reaction equation

HRID 923394 reaction equation
[N+:1]([C:4]1[CH:26]=[CH:25][C:7]([CH2:8][N:9]([CH2:15][C:16]2[CH:21]=[CH:20][C:19]([N+:22]([O-])=O)=[CH:18][CH:17]=2)[C@@H:10]2[CH2:14][CH2:13][O:12][CH2:11]2)=[CH:6][CH:5]=1)([O-])=O.[N+](C1C=CC(CN(CC2C=CC([N+]([O-])=O)=CC=2)C2C=CC=CC=2)=CC=1)([O-])=O>>[NH2:22][C:19]1[CH:18]=[CH:17][C:16]([CH2:15][N:9]([CH2:8][C:7]2[CH:25]=[CH:26][C:4]([NH2:1])=[CH:5][CH:6]=2)[C@@H:10]2[CH2:14][CH2:13][O:12][CH2:11]2)=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 16114856HCID 16114856, compoundHCID 59540143HCID 59540143, compound

Product 1

HCID 59540448HCID 59540448, compoundYield 109%

Procedure

The title compound was prepared using the methods from Example 1B substituting the product from Example 44A for the product from Example 1A to provide the title compound (1.02 g, 109% yield).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-2dec6928d12947ba92cf8eb9be36514e
Source dataset
uspto-grants-2016_03
Patent number
US09278922B2

Reaction notes

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