HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 59540289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | Benzene, 1-(bromomethyl)-3-nitro- | HCID 77568 | — |
| Product | HCID 59540289 | HCID 59540289 | 87% |
Reaction Steps
4-Fluoroaniline and 3-nitrobenzyl bromide were processed using the method described in Example 1A to provide 1.46 g (87%) of the title compound. 1H NMR (400 MHz, DMSO-D6) δ 4.88 (s, 4 H) 6.69-6.75 (m, 2 H) 6.97 (t, J=8.89 Hz, 2 H) 7.64 (t, J=7.81 Hz, 2 H) 7.70-7.74 (m, 2 H) 8.08-8.13 (m, 4 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278922B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-0b4a388f856642379012288854d6c237 |
| Source note | uspto-grants-2016_03 |