HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 82407353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 90079332 | HCID 90079332 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 82407353 | HCID 82407353 | — |
Reaction Steps
To a solution of 2-azido-1-(2-fluoro-4-methoxyphenyl)ethanone (4.80 g, 25.36 mmol) in 100 mL of tetrahydrofuran were added triphenylphosphine (6.65 g, 25.36 mmol) and p-toluenesulfonic acid (14.5 g, 76.11 mmol), followed by stirring at room temperature for 16 hrs.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278996B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-4b11365f7e6b42469a39f8cf328742a4 |
| Source note | uspto-grants-2016_03 |