HuagongsheHuagongshe Chemistry Print Report · For research reference only
(R)-3-Pyrrolidinol → HCID 89907831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (R)-3-Pyrrolidinol | HCID 2759337 | — |
| Reactant | HCID 89906587 | HCID 89906587 | — |
| Product | HCID 89907831 | HCID 89907831 | — |
Reaction Steps
The title compound was prepared in an analogous fashion to that described in Stage 33.1 using 5-bromo-6-chloro-N-(4-((trifluoromethyl)sulfinyl)phenyl)nicotinamide (Stage 222.2) and (R)-pyrrolidin-3-ol to afford an amorphous off-white solid. HPLC (Condition 4) tR=4.83 min, UPLC-MS (Condition 3) tR=0.95 min, m/z=478.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278981B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-477678c8233c4a9eba1a67e754d1bbcd |
| Source note | uspto-grants-2016_03 |