HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Methylphenyl)thiourea → 1-(o-tolylcarbamothioyl)-3-[[3-[1-[4-(trifluoromethoxy)phenyl]-1 H-1,2,4-triazol-3-yl]phenyl]methyl]urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Methylphenyl)thiourea | HCID 2787703 | — |
| Reactant | 3-(3-(isocyanatomethyl)phenyl)-1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazole | HCID 90412150 | — |
| Product | 1-(o-tolylcarbamothioyl)-3-[[3-[1-[4-(trifluoromethoxy)phenyl]-1 H-1,2,4-triazol-3-yl]phenyl]methyl]urea | HCID 90412749 | — |
Reaction Steps
The title compound was prepared as described in Example 75 using 3-(3-(isocyanatomethyl)phenyl)-1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazole (CB34) and 1-(o-tolyl)thiourea and isolated as an off-white solid (0.148 g, 37%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278964B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-f5756f26c0ff4cd8926911fa68e75a26 |
| Source note | uspto-grants-2016_03 |