HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethanol → HCID 19622756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | HCID 86669344 | HCID 86669344 | — |
| Product | HCID 19622756 | HCID 19622756 | 62.5% |
Reaction Steps
Followed procedure described in Intermediate 8, step 1 starting from 3-hydroxy-4-methoxybenzaldehyde and 2-bromoethanol with the reaction conditions of 90° C. overnight. Isolated 400 mg, yield 62.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09283213B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-da3bdb0875c343dfade086408b43bfaf |
| Source note | uspto-grants-2016_03 |