HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,6-Dipropylphenol → 2,6-Dipropyl4-propionylphenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,6-Dipropylphenol | HCID 81107 | — |
| Edukt | Sodium Propionate | HCID 2723816 | — |
| Lösungsmittel | Trifluoromethanesulfonic acid | HCID 62406 | — |
| Produkt | 2,6-Dipropyl4-propionylphenol | HCID 11310872 | — |
Reaktionsschritte
Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07091230B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-ec11d9e4f3f449f6a915145c8ea66bec |
| Quellennotiz | uspto-grants-2006_08 |