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HRID925044

反应详情

EQUATION

反应方程式

HRID 925044 的结构方程式

REACTANTS

反应物

3
结构：CC(C)P(Cl)C(C)C
HCID538967

Chlorodiisopropylphosphine

C6H14ClP

结构：[Li]CCCC
HCID178418339

未命名化合物

结构：CCc1ccccc1NC(=N)c1ccc(C)cc1
HCID178436103

未命名化合物

PRODUCTS

生成物

1
结构：CCc1ccccc1NC(=NP(C(C)C)C(C)C)c1ccc(C)cc1
HCID178436105

未命名化合物

PROCEDURE

实验过程

Procedure as described for NP Amidine I using the following amounts: 1.19 g of N1-(2-ethylphenyl)-4-methylbenzamidine (Amidine VIII, 5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.80 mL chlorodiisopropylphosphine (5.0 mmol). After filtration to remove lithium chloride and removal of solvent, a yellow oil was isolated (1.77 g, 100%).

WORKUP

后处理

  1. filtrationAfter filtration
  2. customto remove
  3. customlithium chloride and removal of solvent
  4. customa yellow oil was isolated (1.77 g, 100%)