HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodiisopropylphosphine → HCID 178460691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodiisopropylphosphine | HCID 538967 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178512003 | HCID 178512003 | — |
| Product | HCID 178460691 | HCID 178460691 | — |
Reaction Steps
Procedure as described for NP Amidine I using the following amounts and modifications: 1.52 g of N1-(2-(phenylthio)phenyl)benzamidine (Amidine XIV, 5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.80 mL chlorodiisopropylphosphine (5.0 mmol). After filtration to remove lithium chloride and removal of solvent, a yellow oil was isolated (2.07 g, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09283555B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-032f5e9147f3446db941515b2d14c893 |
| Source note | uspto-grants-2016_03 |