HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodiphenylphosphine → HCID 178420560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodiphenylphosphine | HCID 66180 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178512003 | HCID 178512003 | — |
| Product | HCID 178420560 | HCID 178420560 | — |
Reaction Steps
Procedure as described for NP Amidine I using the following amounts and modifications: 1.34 g of N1-(2-(phenylthio)phenyl)benzamidine (Amidine XIV, 4.4 mmol), 2.20 mL of 2.0 M butyllithium (4.4 mmol), 0.78 mL chlorodiphenylphosphine (4.4 mmol). After filtration to remove lithium chloride and removal of solvent, a sticky solid was isolated (2.01 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09283555B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-3327e8f5da3c48779a5b777c095dcf02 |
| Source note | uspto-grants-2016_03 |