HCID 86725349, compound → HCID 86725351, compound

Participants

Reaction Conditions

Reaction Steps

The product from step (b) (1.13 mmol) was dissolved in 4N HCl/dioxane and heated to 60° C. for 1 hour after which time LCMS indicated no starting material. The reaction mixture was cooled to RT and the solvent was evaporated in vacuo to give the crude product as a brown semi-solid. Purification by flash silica-gel chromatography (gradient elution: 0-50% EtOAc in hexanes) gave the sub-title compound (22 mg) as a yellow oil. MS: ESI (positive): 365 (M+H).

Provenance & Evidence