HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → 3-(2-Azidoethyl)-5,6-dichloro-2-(triethylsilyl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 86699391 | HCID 86699391 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-(2-Azidoethyl)-5,6-dichloro-2-(triethylsilyl)-1H-indole | HCID 86699392 | — |
Reaction Steps
3-(2-azidoethyl)-5,6-dichloro-2-(triethylsilyl)-1H-indole was prepared according to method D Step IV with 3-(2-bromoethyl)-5,6-dichloro-2-(triethylsilyl)-1H-indole (0.548 g; 1.35 mmol) and sodium azide (0.262 g; 4.04 mmol) in DMF (8 mL); the yield was quantitative as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09284271B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-fd126041eba64373bb03c3c91d249646 |
| Source note | uspto-grants-2016_03 |