(4-Methoxyphenyl)boronic acid → HCID 72943318, compound

Participants

Reaction Steps

The title compound, off-white solid (65 mg, 82%), MS (ISP) m/z=318.4 [(M+H)+], mp 278.5° C., was prepared in accordance with the general method of example 1 from 6-bromo-1-oxo-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole-8-carbonitrile (intermediate 15) (72.5 mg, 0.25 mmol) and commercially available 4-methoxy-phenylboronic acid (49.4 mg, 0.325 mmol).

Provenance & Evidence