3-Fluorophenylboronic acid → HCID 118341188, compound

Participants

Reaction Steps

The title compound, white solid (61 mg, 78%), MS (ISP) m/z=313.6 [(M+H)+], mp 222° C., was prepared in accordance with the general method of example 1 from 6-bromo-8-fluoro-10-methyl-3,4-dihydro-2H-pyrazino[1,2-a]indol-1-one (intermediate 14) (74.3 mg, 0.25 mmol) and commercially available 3-fluoro-phenylboronic acid (45.5 mg, 0.325 mmol).

Provenance & Evidence