HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-methylbenzeneboronic acid → HCID 118341129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-methylbenzeneboronic acid | HCID 2782674 | — |
| Reactant | HCID 90036013 | HCID 90036013 | — |
| Product | HCID 118341129 | HCID 118341129 | — |
Reaction Steps
The title compound, off-white solid (69 mg, 81%), MS (ISP) m/z=343.4 [(M+H)+], mp 225° C., was prepared in accordance with the general method of example 1 6-bromo-8-chloro-10-methyl-3,4-dihydro-2H-pyrazino[1,2-a]indol-1-one (intermediate 12) (78.4 mg, 0.25 mmol) and commercially available 3-fluoro-4-methyl-phenylboronic acid (50.0 mg, 0.325 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09284321B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-bd3cca0ed272448a9420541d0b8feba7 |
| Source note | uspto-grants-2016_03 |