3-Pyridinylboronic acid → HCID 73335615, compound

Participants

Reaction Steps

The title compound, off-white solid (50 mg, 69%), MS (ISN) m/z=289.4 [(M+H)+], mp 272.5° C., was prepared in accordance with the general method of example 1 from 6-bromo-1-oxo-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole-8-carbonitrile (intermediate 15) (72.5 mg, 0.25 mmol) and commercially available pyridin-3-ylboronic acid (39.9 mg, 0.325 mmol).

Provenance & Evidence